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q?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>(Ni3S2/Ni/NF)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>一U?/span>?/span>?/span>?/span>{?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Ni3S2/Ni Heterostructure Nanobelt Arrays as Bifunctional Catalysts for Urea-Rich Wastewater Degradation?/span>?/span>?/span>?/span>?/span>ACS Applied Materials & Interfaces?/span>?/span>


Ni3S2?/span>Ni?/span>?/span>?/span>?/span>?/span>l?/span>?/span>所?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Ni?/span>U?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>OH??/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>NiOOHQ?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>_?/span>l?/span>?/span>?/span>2DU?/span>c?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>UORQ?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>HERQ?/span>?/span>?10 mA cm?2?/span>?/span>?/span>?/span>?/span>所?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>1.30 V?/span>?54 mV?/span>?/span>需1.36 V?/span>?/span>?/span>10 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>100 mA cm?2E?/span>?/span>?/span>?/span>60?/span>?/span>?/span>



?/span>1. Ni3S2/Ni/NF?/span>?/span>?/span>C?/span>?/span>?/span>?/span>

?/span>2. Ni3S2/Ni/NF?/span>(a-b) SEM?/span>?/span>Q?/span>(c-e) HRTEM?/span>?/span>?/span>(f-i) HADDF-STEM?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


?/span>3. Ni3S2/Ni/NF?/span>(a) XRD?/span>?/span>?/span>(b) XPS?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>XPS?/span>?/span>Q?/span>(c) Ni 2p?/span>(d) S2p?/span>

?/span>4. (a) Ni3S2/Ni/NF?/span>UOR?/span>OER?/span>?/span>?/span>U?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>(b) UOR?/span>?/span>?/span>U?/span>Q?/span>(d) Tafel?/span>?/span>?/span>(e) Nyquist?/span>Q?/span>(c) Ni3S2/Ni/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>10 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>UORz?/span>?/span>?/span>?/span>?/span>Q?/span>(f) Ni3S2/Ni/NF?/span>UORE?/span>?/span>?/span>?/span>



?/span>5. (a) Ni3S2/Ni/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>HER?/span>?/span>?/span>U?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>(b) HER?/span>?/span>?/span>U?/span>Q?/span>(c) Tafel?/span>?/span>?/span>(d) Nyquist?/span>Q?/span>(e) Ni3S2/Ni/NF?/span>HERE?/span>?/span>?/span>Q?/span>(f) ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>10~100 mV s?1?/span>Cdl?/span>?/span>


?/span>6. (a) ?/span>?/span>?/span>?/span>?/span>?/span>C?/span>?/span>?/span>Q?/span>(b) Ni3S2/Ni/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>Q?/span>(c) ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>Q?/span>(d) Ni3S2/Ni/NF?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>Q?/span>(e) Ni3S2/Ni/NF?/span>最q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>10 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>


?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>ACS Applied Materials & Interfaces?/span>Q?/span>DOIQ?/span> 10.1021/acsami.1c08148?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>W?/span>一?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>{?/span>?/span>?/span>?/span>?/span>?/span>?/span>


?/strong>?/strong>?/strong>?/strong>

https://doi.org/10.1021/acsami.1c08148

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